Formulation Advisory Cosmetic Testing Service
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Formulation Advisory Cosmetic Testing Service
Home
About Us
Testing Capabilities
Enquiries & Appointments
Additional Information
Our Partners
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Cosmetic Stability Testing

Preliminary, Accelerated & Real Time Stability

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Preservative Efficacy Testing

Microbiological Testing To Check Your Preservative

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Water Analysis

A Wide Range Of Analyses To Check Water Quality

Testing Capabilities

Additional Information

COSMETIC STABILITY TESTING

The purpose of stability testing is to ensure the product maintains its intended physical, chemical, and microbiological quality, as well as functionality and aesthetics when stored under the appropriate conditions.  At selected intervals, samples are evaluated for various physical, chemical and performance characteristics to see if and how they have changed.  The product must remain stable and any sign of instability is evaluated to determine if reformulation may be required.


Tests offered include:

  • Preliminary Stability Testing - 14 days
  • Accelerated Stability Testing - 3 to 6 months
  • Real Time Stability Testing - Up to 3 years
  • Freeze Thaw and Thermal Cycling Studies - 6 Cycles


We have the capabilities to test organoeliptical properties such as colour, odour & appearance; physiochemical properties such as pH, viscosity and density, microbial count; container compatibility and emulsion creaming.  Finished product samples are evaluated against a standard sample and with reference products subjected to the same test conditions.  The amount of product required will depend on your testing protocol. Testing may also be performed on raw material samples.


PRESERVATIVE  EFFICACY TESTING

Preservative efficacy testing checks your product to see how the preservative system copes when challenged by different types of bacteria over 28 days.  The microbes of known type and concentration are added to your product, then samples are taken on days 0, 7, 14, and 28 and evaluated.  A good result is when no microbes grow, or when tested according to the relevant standards, the preservative reduces the number of colony forming units over time.  The microbes used in this test are Pseudomonas aeruginosa, Staphylococcus aureus, Escherichia coli, Candida albicans, Aspergillus brasiliensis. We can also challenge with a Bacillus species to evaluate your preservative's effectiveness against spore forming microorganisms.  Re-challenge testing is also available.


MICROBIOLOGICAL ANALYSIS

We offer one-off single microbiological tests to evaluate raw materials, finished products, packaging, environments, equipment and surfaces for yeast, mould and total bacteria.  This testing is very useful for checking the quality of raw materials and for testing bulk product during manufacturing. To allow time for the growth of fungi, the results of these tests are usually available after 7 days.


TIME KILL TESTS

The effectiveness of antimicrobial agents incorporated into disinfectants, sanitisers and antiseptics is measured by their ability to kill microorganisms within a specified contact time.  To accurately determine this, complete and immediate inactivation (neutralisation) of the antimicrobial agent is required.  Inefficient inactivation could allow the agent to continue killing the microorganisms beyond the exposure time and this would result in an over estimation of antimicrobial activity.


A time kill test measures the changes in a population of aerobic microorganisms over time, after exposure to a test material.  The test material e.g. finished product, is brought into contact with a known population of microorganisms for a specific period.  A neutralisation technique is applied to quench or stop the antimicrobial activity of the test material at different sampling intervals.  The surviving microorganisms are then counted.  The time taken to complete this test because the method for quenching the antimicrobial agent has to be determined and proven to be effective for each material tested, against each microorganism selected for the test. The procedure becomes more complex and time consuming when additional types of microorganisms are included in the test.


WATER QUALITY TESTING

Water is a major component in many formulations.  It is also used in preparatory processes such as rinsing glassware, and other materials.  Using the right kind and quality water is essential for ensuring product quality.  Whether it be purified, demineralised spring water or distilled water, it is highly recommended you have a sample tested to verify its quality.  Typical water tests include conductivity & microbiological analysis.  Other tests may be performed on request.



Oil Acidity & Peroxide Testing Capabilities

Peroxide & Acid Values of Vegetable Oils

Our laboratory uses CDR FoodLab® to test the quality of nut, seed and other vegetable oils.  It is also used to test the quality of essential oils.  A certificate of analysis is provided for each set of samples analysed. Peroxide and acid value determinations may be performed on raw materials to check their quality prior to production, or to obtain additional scientific data to support expiry date extensions.  For finished products that contain a large amount of vegetable oils, our stability testing regime (accelerated and real time) now includes the assessment of peroxide values.  


The amount of peroxides indicates the degree of primary oxidation and therefore the likeliness of becoming rancid.  Generally, a lower number of peroxides indicates a good quality of oil, and a good preservation status.  Unsaturated free fatty acids react with oxygen and form peroxides, which result in a series of chain reactions that generate volatile substances. Those reactions are accelerated by high temperature and by light and oxygen exposure.  The CDR method for the determination of peroxide value of oils and fats showed very good correlation with the reference method:AOCS Official Method cd 8-53. In addition, the international reference laboratory Campden BRI carried out comparative tests between the CDR FoodLab® method for determining the peroxide value and the UKAS accredited titration method used by Campden BRI (Campden BRI Method TES-AC-360 based on ISO 3960 or AOCS Cd 8b-90 or  AOAC 965.33): the correlation coefficient was R² = 0.9681, a value that shows that very good correlation between the two methods.


The acid content of fats is given by the quantity of free fatty acids deriving from the hydrolytic rancidity of triglycerides. As this alteration occurs in unsuitable conditions for the processing and preservation of fats, acidity represents a basic indicator of the genuineness of the product. The test is particularly important during the refining of oils and fats, for the assessment of the processing cycle and for the definition of product categories. This test has the same accuracy as the AOCS Official Method Ca 5a-40.


We offer discounted testing rates for oils requiring multiple analyses.  Currently we can analyse in-house for peroxide, acidity, refractive index, microbial content and moisture content (loss on drying).
 

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